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Spherical Electrochemical Corrosion Test Cell with Luggin Capillary and Specimen Holder

Standard & Customized Electrochemical Cells

Spherical Electrochemical Corrosion Test Cell with Luggin Capillary and Specimen Holder

Item Number : PL-DJ18

Price varies based on specs and customizations


Exposed Specimen Area
1.0 cm²
Standard Volume Options
500 mL / 1000 mL
Salt Bridge Solution
Saturated Potassium Nitrate (KNO3)
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Product Overview

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This high-performance spherical electrochemical corrosion test cell is engineered to meet the stringent demands of modern materials science, metallurgy, and electrochemical research. Designed to facilitate precise, reproducible, and highly controllable corrosion testing, this system provides an ideal environment for investigating the electrochemical behavior of metallic specimens in various aggressive liquid media. The spherical geometry of the glass vessel is specifically optimized to ensure uniform current density distribution across the electrolyte, which is a critical factor in achieving reliable Tafel plots, polarization resistance measurements, and cyclic voltammetry data.

At the core of this equipment's value proposition is its ability to minimize experimental errors that commonly plague standard corrosion testing setups. By integrating an adjustable-angle Luggin capillary salt bridge and a standardized specimen holder, the unit drastically reduces ohmic resistance ($IR$ drop) and eliminates stray crevice corrosion. The system is widely utilized in industrial R&D centers, quality control laboratories, and academic institutions worldwide, serving industries such as oil and gas, petrochemical processing, aerospace, marine engineering, and infrastructure development.

Built with premium, chemically resistant materials, this system offers outstanding durability and operational longevity under demanding laboratory conditions. Every glass component is crafted from high-purity borosilicate glass, while all sealing, structural, and mounting components are manufactured from custom CNC-machined polytetrafluoroethylene (PTFE). This precise material selection guarantees exceptional resistance against organic solvents, strong acids, and hot electrolytes, ensuring that researchers can perform high-temperature and highly corrosive experiments with absolute confidence in the mechanical and chemical integrity of their apparatus.

Key Features

  • Adjustable-Angle Luggin Capillary (Salt Bridge): The integrated salt bridge is designed with an adjustable-angle mechanism, allowing researchers to position the tip of the Luggin capillary extremely close to the working electrode surface. This precise alignment minimizes the electrolyte path length between the reference and working electrodes, effectively reducing the $IR$ drop for highly accurate potential measurements.
  • Chloride-Free Electrolyte Isolation: To prevent exogenous chloride ion contamination from interfering with sensitive corrosion studies, the salt bridge is designed to be filled with a saturated potassium nitrate ($KNO_3$) solution, ensuring clean electrochemical reactions without compromising the integrity of the reference system.
  • Precision Defined-Area Specimen Holder: The working electrode assembly features a robust specimen holder that accommodates 14mm diameter metal samples. By utilizing a highly engineered sealing gasket, the holder exposes an exact, standardized area of 1.0 cm² to the corrosive fluid, preventing crevice corrosion at the sample edges and ensuring consistent current density calculations.
  • Dual-Phase F-Type Gas Purging System: This apparatus features a versatile F-type gas inlet tube that allows users to bubble inert purging gases (such as high-purity nitrogen or argon) directly below the liquid level to remove dissolved oxygen prior to testing. During active measurements, the gas flow can be switched to the headspace to maintain a stable, non-reactive blanketing atmosphere without introducing convective noise to the cell.
  • Advanced PTFE and Ground-Glass Sealing: The cell incorporates a high-precision ground glass neck that pairs seamlessly with a tapered PTFE lid, establishing a tight, hermetic seal. Furthermore, the electrode ports on the lid utilize O-ring compression screws, ensuring that volatile solvents do not evaporate during long-term exposure and isolating the cell from atmospheric oxygen.
  • Jacketed and Single-Layer Structural Variants: To accommodate various temperature-dependent studies, the cell is available in both single-layer and double-layer jacketed configurations. The jacketed version allows a constant-temperature fluid from a circulating water or oil bath to flow through the outer chamber, keeping the internal electrolyte at a highly stable temperature.
  • Expandable Multi-Port Design: The standard configuration provides a 5-port lid design to house the working electrode, counter electrode, reference electrode salt bridge, gas inlet, and gas outlet. For jacketed configurations requiring real-time temperature tracking, the cell body can be customized with an additional dedicated port to accommodate an external thermometer or PT100 sensor, transforming it into a highly functional 6-port vessel.

Applications

Application Description Key Benefit
Alloy Pitting & Crevice Evaluation Characterizing the susceptibility of stainless steels and nickel alloys to localized corrosion in acidic or halide-bearing solutions. Precision-defined 1.0 cm² exposure area prevents edge-effect crevice corrosion, ensuring reliable pitting potential data.
Corrosion Inhibitor Screening Evaluating the efficiency of organic and inorganic chemical inhibitors added to simulated industrial water systems or oilfield brines. F-type gas purging permits rapid de-aeration to simulate anaerobic pipeline conditions with high repeatability.
Marine Material Optimization Simulating long-term exposure of structural marine alloys, coatings, and surface treatments in synthetic seawater environments. High borosilicate glass and PTFE construction resist aggressive saltwater solutions without leaching trace elements.
Petrochemical Process Simulation Testing metal specimens under hot acidic conditions simulating refinery distillation columns and chemical reactors. Jacketed outer wall enables precise temperature control from room temperature up to 150°C using silicone oil.
Electrochemical Impedance Spectroscopy Performing high-frequency AC impedance sweeps to study the passivation kinetics and oxide film growth on metals. The adjustable Luggin capillary minimizes solution resistance, preventing high-frequency phase shifts and artifacts.
Acid Rain & Atmospheric Simulation Investigating the atmospheric degradation of architectural metals and coated steels using sulfurous or nitrous simulated acid rain. Saturated $KNO_3$ salt bridge prevents chloride contamination, isolating the exact chemical influence of acid rain anions.

Technical Specifications

Parameter Description / Specification Details
Model Number PL-DJ18 Universal Reference Code
Standard Volume Options 500 mL / 1000 mL Custom volumes available upon request
Vessel Material High Borosilicate Glass 3.3 Low thermal expansion, high optical clarity
Lid & Stopper Material Pure Polytetrafluoroethylene (PTFE) Superior chemical inertness and CNC accuracy
Vessel Configuration Single-Layer (Standard) / Double-Layer (Jacketed) Jacketed model supports circulating water/oil baths
Working Electrode Sample Diameter 14 mm Flat disc specimen geometry
Exposed Specimen Area 1.0 cm² Standardized for current density calculation
Salt Bridge Assembly Adjustable-angle Luggin capillary Reduces $IR$ drop during polarization sweeps
Salt Bridge Solution Saturated Potassium Nitrate ($KNO_3$) Chloride-free salt bridge design
Gas Inlet Configuration F-type dual-phase purging tube Sub-surface bubbling and head-space blanketing
Sealing Interfaces Ground-glass joint with tapered PTFE lid Threaded compression O-ring seals for electrodes
Temperature Range Room Temperature to 90°C (Water) / 150°C (Oil) Supported on jacketed variants
Port Configuration 5-Port (Standard) / 6-Port (Optional) 6-Port option adds thermometer port to cell body
Included Components Glass Cell Body, F-Type Gas Inlet, Salt Bridge, Liquid Seal, PTFE Stopper Set, Specimen Holder, Graphite Rod Electrode Comprehensive kit for immediate electrochemistry
Chemical Compatibility Highly compatible with organic solvents and mineral acids Strictly exclude Hydrofluoric Acid (HF)

Why Choose This Product

Choosing this electrochemical cell means investing in premium engineering that translates directly to high-fidelity, publishable, and industrially valid research data. Unlike standard, mass-produced glassware, our vessels are fabricated from premium borosilicate 3.3 glass that undergoes rigorous thermal annealing to relieve internal mechanical stresses, preventing cracking during high-temperature cycles. The high-density PTFE components are custom CNC-machined rather than molded, delivering tight mechanical tolerances that ensure perfect hermetic sealing and a long service life without degradation.

Furthermore, KINTEK's end-to-end manufacturing capability allows us to easily customize standard configurations to align with your unique laboratory setup. Whether you require a specialized 6-port vessel body with integrated thermocouple wells, larger custom volumes, or specialized working electrode adapter rods for alternative sample sizes, our engineering team can fabricate bespoke components to your exact specifications. By selecting our premium corrosion cell, B2B procurement teams and research scientists are guaranteed a reliable, highly adaptable instrument backed by responsive technical support and a comprehensive warranty program.

Please contact our sales and engineering team today to receive a detailed quote or to discuss custom modifications for your specific electrochemical research needs.

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Product Datasheet

Spherical Electrochemical Corrosion Test Cell with Luggin Capillary and Specimen Holder

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Standard & Customized Electrochemical Cells


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