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H Type Replaceable Membrane Electrochemical Cell for Three Electrode System Jacketed Single Layer Gas Purging

Standard & Customized Electrochemical Cells

H Type Replaceable Membrane Electrochemical Cell for Three Electrode System Jacketed Single Layer Gas Purging

Item Number : PL-DJ01

Price varies based on specs and customizations


Chamber Volume Options
30 mL to 500 mL (Customizable)
Material Composition
High Borosilicate Glass & PTFE
Temperature Control
Jacketed Constant Temperature Water Bath (Optional)
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Product Overview

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This H-type replaceable membrane electrochemical cell represents the pinnacle of modular laboratory reactor design, engineered to facilitate high-precision divided-cell electrolysis and multi-electrode analytical testing. Designed for researchers requiring strict isolation between anodic and cathodic half-reactions, this system maintains low ohmic resistance and prevents cross-contamination.

Commonly utilized in clean energy research and organic synthesis, this system is optimized for applications like carbon dioxide reduction, nitrogen fixation, and electro-catalyst evaluation. It serves research laboratories and industrial R&D centers focusing on battery technology, corrosion studies, and advanced electrolysis.

Manufactured to withstand demanding laboratory conditions, this unit utilizes high borosilicate glass and precision-machined fluoropolymer sealing components to ensure outstanding thermal stability and chemical resistance. This robust construction delivers consistent, repeatable results under continuous gas-purging conditions.

Key Features

  • Modular Divided-Chamber Architecture: The dual-chamber configuration is split into distinct cathode (working electrode) and anode (counter electrode) compartments, separated by a user-provided ion-exchange membrane. A robust mechanical chain clamp provides consistent circumferential pressure across the interface, ensuring a leak-tight seal while allowing rapid membrane replacement without altering the cell's physical geometry.
  • Optimized Low IR Drop Design: To minimize solution resistance (IR drop) and ensure highly accurate potential control, the reference electrode is positioned in the same chamber as the working electrode. This close physical proximity mitigates the ohmic resistance of the electrolyte path, ensuring precise potentiostatic and galvanostatic measurements during sensitive electrochemical trials.
  • 360-Degree Rotatable PTFE Port Inserts: The glass entry ports are designed with external threads and host an inner core crafted from premium, CNC-machined polytetrafluoroethylene (PTFE) that rotates a full 360 degrees. This allows operators to achieve precise angular alignment of the elongated electrodes, keeping them perfectly parallel to the membrane surface for uniform current density.
  • Advanced Gas Purge and Aeration Systems: The cell features integrated sub-surface gas delivery tubes tailored for specific gas-liquid reactions. Standard straight-tube purgers facilitate carbon dioxide reduction processes, while specialized L-shaped gas purge tubes are included for nitrogen reduction experiments, optimizing bubble distribution and mass transfer.
  • Hermetic Compression Sealing System: Electrode integration is secured via heavy-duty PTFE plugs utilizing a specialized compression mechanism. By tightening the external POM caps against high-durability fluoropolymer O-rings, the system achieves a highly reliable, leak-free relative seal, protecting volatile electrolytes and sensitive reactions from atmospheric exposure.
  • Overhead Dead-Volume Prevention: The single-layer glass vessel incorporates an innovative elevated base design. This smart structural geometry raises the active solution volume above potential dead zones, preventing fluid entrapment and ensuring homogeneous mixing and complete recovery of valuable target compounds.
  • Jacketed Thermal Regulation Options: Available in both single-layer and double-layer configurations, the jacketed variant integrates an outer jacket for external water bath circulation. This allows researchers to continuously pump temperature-controlled fluid around the active volume, maintaining strict isothermal conditions for thermodynamic studies.
  • Flexible, Scalable Chamber Volumes: Standard models range from 30 mL to 500 mL capacities to accommodate varying sample sizes, with specialized 10 mL versions utilizing a unique internal thread design. Additionally, the cell body can be customized to include auxiliary sampling ports, allowing real-time fluid withdrawal without disrupting the internal atmosphere.

Applications

Application Description Key Benefit
Carbon Dioxide Reduction ($CO_2RR$) Investigating the electrocatalytic conversion of carbon dioxide into high-value chemical feedstocks and synthetic fuels using gas-diffusion setups. Straight gas purge tubes maximize gas-liquid boundary layer interaction for high Faradaic efficiency.
Nitrogen Reduction Reaction ($NRR$) Conducting ambient-pressure ammonia synthesis from nitrogen and water, requiring highly controlled atmospheres and pristine chemical purity. L-shaped gas purge tubes ensure uniform bubble distribution across the catalyst surface, preventing nitrogen mass transport limitations.
Electrocatalyst Evaluation Characterizing the activity, stability, and selectivity of novel catalytic materials in a three-electrode configuration under controlled conditions. Minimized IR drop and parallel electrode alignment yield highly accurate polarization curves and cyclic voltammetry data.
Organic Electrosynthesis Performing selective synthetic organic transformations at anode or cathode compartments while isolating reactive intermediates from the counter electrode. Complete physical separation of chambers prevents undesired cross-reactions and side-product formation at the opposite electrode.
Hydrogen Evolution Reaction (HER) Evaluating catalyst performance and proton exchange kinetics during electrochemical water splitting under acidic or alkaline conditions. Heavy-duty chain-clamped membrane interface resists pressure fluctuations while providing low ionic resistance for proton transport.
Corrosion and Passivation Studies Monitoring the electrochemical behavior and degradation rates of advanced alloys and protective coatings exposed to aggressive electrolytes. High borosilicate glass and fluoropolymer seals resist highly corrosive acid/base media, ensuring zero contamination of the sample.

Technical Specifications

Parameter / Specification PL-DJ01 (Standard) PL-DJ01-2 (Absolute Sealed) PL-DJ01-10 (Micro-Volume)
Base Architecture Dual-chamber H-type with elevated layer Dual-chamber H-type absolute seal Compact micro-volume dual chamber
Chamber Capacity Range 30 mL, 50 mL, 100 mL, 150 mL, 250 mL, 500 mL (Customizable) 30 mL to 500 mL 10 mL (Fixed)
Sealing Mechanism Relative seal via POM external cap & PTFE compression plug Absolute gas-tight hermetic compression Threaded joint interface with PTFE plugs
Port Thread Style External thread High-precision compression thread Internal thread
Electrode Compatibility Requires elongated working, auxiliary, and reference electrodes Requires elongated working, auxiliary, and reference electrodes Sub-miniature or custom elongated electrodes
Chamber Separation Ion-exchange membrane (user-supplied) with chain clamp Ion-exchange membrane (user-supplied) with chain clamp Integrated membrane slot with mechanical lock
Gas Aeration System Sub-surface straight (for $CO_2$) or L-shape (for $N_2$) Sub-surface straight (for $CO_2$) or L-shape (for $N_2$) Micro-gas dispersion tube
Temperature Regulation Available in Single-Layer or Jacketed Double-Layer (water bath circulation) Available in Single-Layer or Jacketed Double-Layer (water bath circulation) Single-Layer standard
Glass Body Design High borosilicate glass with elevated base structure High borosilicate glass with elevated base structure High borosilicate glass with space-efficient profile
Optional Modifications Customizable sampling ports, custom volumes Customizable sampling ports, custom volumes Custom ports upon request

Why Choose This Product

  • Uncompromised Materials & Craftsmanship: Every component is constructed from premium high-borosilicate glass and medical-grade PTFE, CNC-machined to exacting tolerances to resist corrosive acids, organic solvents, and extreme temperatures.
  • Enhanced Measurement Precision: By positioning the reference electrode in the same chamber as the working electrode and allowing 360-degree rotational alignment, the system significantly reduces IR drop and current distribution errors.
  • Outstanding Experimental Flexibility: With modular single-layer, jacketed, and specialized micro-volume options, alongside custom sampling ports and tailored gas purging setups, the unit adapts seamlessly to a vast array of experimental conditions.
  • Superior Sealing Integrity: The mechanical chain clamp combined with screw-compressed O-ring PTFE seals ensures a secure relative seal, preventing gas leakage and preserving the integrity of oxygen-sensitive or volatile chemical reactions.
  • End-to-End Technical Support & Customization: Backed by KINTEK's comprehensive custom manufacturing capabilities, we can modify chamber shapes, dimensions, and port configurations to match your exact experimental requirements.

Contact KINTEK's technical sales team today to request a quote or discuss a custom-engineered electrochemical cell configuration tailored to your laboratory's exact specifications.

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H Type Replaceable Membrane Electrochemical Cell for Three Electrode System Jacketed Single Layer Gas Purging

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Standard & Customized Electrochemical Cells


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