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Replaceable Membrane H Type Electrochemical Cell for Three Electrode Gas Aeration Experiments

Standard & Customized Electrochemical Cells

Replaceable Membrane H Type Electrochemical Cell for Three Electrode Gas Aeration Experiments

Item Number : PL-DJ08

Price varies based on specs and customizations


Standard Volume
10 mL
Chamber Junction Design
Integrated Luggin Capillary
Sealing Configurations
Relative Sealing and Absolute Sealing Options
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Product Overview

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This advanced replaceable membrane electrochemical cell represents a significant evolution in H-type cell design, specifically engineered to meet the stringent demands of modern electrochemical research. By dividing the system into distinct working and counter electrode compartments separated by an easily replaceable membrane, this system minimizes cross-contamination and allows for precise control of half-cell reactions. The integration of a built-in Luggin capillary directly at the junction of the reference and working electrode chambers solves a major pain point in traditional designs by significantly reducing solution resistance and ohmic drop during testing.

Ideal for a wide range of applications, this equipment is the preferred choice for researchers in electrocatalysis, lithium-ion battery development, hydrogen evolution reactions, and carbon dioxide reduction. Its dual-chamber design makes it uniquely suited for systems requiring absolute separation of anodic and cathodic products, such as photoelectrochemical water splitting and redox flow battery membrane crossover studies. Industrial procurement teams and academic research labs alike rely on this unit to deliver highly reproducible cyclic voltammetry, linear sweep voltammetry, and electrochemical impedance spectroscopy data.

Built with absolute confidence in long-term reliability, the cell body is fabricated from premium high borosilicate glass, known for its exceptional chemical inertness and resistance to thermal shock. Paired with our precision-machined polytetrafluoroethylene (PTFE) sealing components, this cell guarantees leak-free operation and maintains structural integrity even under highly acidic, basic, or volatile organic solvent environments. Every unit undergoes rigorous quality control to ensure that your lab receives an instrument capable of executing highly sensitive, trace-level electrochemical analyses without background interference.

Key Features

  • Precision-Engineered Luggin Capillary: An integrated Luggin capillary is strategically positioned at the junction between the reference and working electrode chambers. This unique geometry allows the reference electrode probe to be placed in extremely close proximity to the working electrode surface, drastically reducing the internal resistance (IR) drop to ensure that the measured potential reflects the true interfacial potential at the working electrode.
  • User-Friendly Replaceable Membrane Interface: The dual-chamber structure uses a specialized chain clamp configuration to secure the junction between the cathode and anode compartments. This design allows researchers to easily insert, align, and replace user-supplied ion-exchange membranes within seconds. The reliable mechanical pressure applied by the chain clamp ensures a uniform, leak-proof seal across the membrane surface, preventing electrolyte bypassing.
  • Suspended Single-Layer Cell Architecture: The cell body features a high-clearance, elevated single-layer structure. Unlike conventional glass cells with flat bottoms that can trap droplets or accumulate trace residues in hard-to-clean crevices, this suspended design eliminates hidden solution zones, facilitating complete draining and thorough cleaning between trials.
  • Dual Sealing Adaptability: To accommodate diverse experimental requirements, this system is offered in both relative and absolute sealing configurations. The relative sealing system is ideal for standard reactions where mild atmosphere isolation is sufficient, while the absolute sealing configuration is engineered for air-sensitive, oxygen-free, or highly volatile reactions, offering a totally closed environment.
  • Threaded PTFE Compression Seals: The interface between the glass ports and the electrode components features high-precision internal threads. By tightening the robust, CNC-machined PTFE caps, the system applies controlled vertical force to squeeze high-performance elastomer sealing rings, providing a highly reliable gas-tight and liquid-tight seal without applying excessive stress to the glass.
  • Advanced Electrode Integration and Sealing Options: Depending on the sealing configuration chosen, the electrode entry points are engineered for absolute integrity. For relative sealing, the system utilizes high-performance PTFE plugs with compression screws to deform the O-rings around the elongated electrodes. For absolute sealing, the cell features an innovative PTFE cover with integrated internal headphone-jack style sockets, allowing the electrodes to plug directly inside the cell structure for an impenetrable seal.
  • Sub-Surface Gas Purging and Aeration Assembly: The system includes a dedicated gas inlet tube that extends below the liquid level, allowing for direct bubbling of inert or reactive gases into the electrolyte. This allows for rapid deaeration or the precise establishment of a gas-saturated environment, which is critical for gas-involving reactions like electrochemical carbon dioxide reduction.
  • Scalable Customization and Sampling Port Integration: For laboratories requiring intermediate product analysis, the glass body can be customized with an additional sampling port. This port allows for the extraction of liquid samples at specified intervals during long-term electrolysis runs without disrupting the internal pressure or atmospheric composition.

Applications

Application Description Key Benefit
Electrochemical CO2 Reduction Utilizing the cell to reduce carbon dioxide into high-value chemical feedstocks at the working electrode while keeping the generated oxidation products isolated in the counter chamber. Prevents re-oxidation of gaseous and liquid products at the anode, while the sub-surface gas purge maintains CO2 saturation.
Water Splitting (HER / OER) Conducting separate Hydrogen Evolution Reaction (HER) and Oxygen Evolution Reaction (OER) testing, requiring clean gas collection and high ionic transport. Integrated Luggin capillary minimizes the high IR drop commonly associated with high-current water electrolysis, ensuring accurate overpotential data.
Redox Flow Battery R&D Testing active electrolyte materials, calculating charge-discharge kinetics, and evaluating crossover rates of redox couples across various membrane materials. Quick-change chain clamp permits rapid screening of different ion-exchange membranes without complete disassembly of the cell components.
Photoelectrochemical Catalysis Evaluating semiconductor photoanodes or photocathodes under light illumination when combined with external light sources. Highly transparent borosilicate glass allows maximum light transmission, while the separate chambers isolate generated photo-products.
Electrochemical Corrosion Testing Monitoring the corrosion rates and passivation curves of metal alloys in aggressive acidic or saline media under specific gas blankets. Absolute sealing prevents atmospheric oxygen contamination, enabling accurate measurement of anaerobic corrosion rates.
Organic Electrosynthesis Performing selective synthetic organic chemistry where anodic oxidation and cathodic reduction must proceed in separate compartments to prevent side reactions. Premium PTFE and borosilicate construction provides exceptional chemical resistance against harsh organic solvents and strong electrolytes.

Technical Specifications

Parameter Specification Details
Product Model Number PL-DJ08
Standard Volume 10 mL
Chamber Configuration Dual-chamber 3-H configuration (Cathode and Anode chambers)
Cell Body Material High borosilicate glass (Single-layer with elevated/suspended design)
Design Heritage Upgraded from base model C007-10 with integrated Luggin capillary at the junction
Chamber Connection Heavy-duty chain clamp for rapid membrane replacement
Membrane Requirement User-supplied ion-exchange membrane
Electrode Compatibility Extended / elongated electrodes (Working, Counter, and Reference)
Relative Sealing Method PTFE plug with compression screw to squeeze O-rings
Absolute Sealing Method PTFE cover with internal headphone-jack style plug connections
Glass Port Sealing Internal thread design with PTFE compression elements
Aeration Integration Sub-surface gas purging tube included for atmospheric control
Custom Sampling Port Available as an optional modification (additional fees apply)
Valve Integration Not supported; gas connections utilize quick-connect fittings
Quick-Connect Tubing Size Compatible with 3 mm outer diameter PTFE tubing

Why Choose This Product

  • Premium Material Selection: Crafted from premium high borosilicate glass and high-purity, CNC-machined PTFE. We guarantee that all materials are free from trace contaminants, providing superior resistance to chemical degradation and thermal stress.
  • Advanced Ohmic Compensation: The integration of the Luggin capillary directly into the chamber junction provides unmatched accuracy in potential control, eliminating the need for complex mathematical IR compensation during high-current operations.
  • Uncompromising Leak Tightness: With dual options for relative and absolute sealing, this cell provides an airtight environment that is critical for highly sensitive anaerobic studies. The quick-connect fittings and headphone-style plugs prevent ambient gas ingress.
  • Tailored Customization Capabilities: Backed by our end-to-end CNC machining capabilities, we can modify the cell body to include extra sampling ports, specific cell volumes, or specialized electrode mounts to fit your unique experimental parameters.
  • Optimized for Rapid Workflow: The combination of internal threads, O-ring compression seals, and a fast-acting chain clamp minimizes the time spent setting up and cleaning, allowing researchers to maximize their experimental throughput.

For standard or fully customized setups tailored to your exact experimental parameters, please contact KINTEK today to receive a detailed quote or consult with our technical engineering team.

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Replaceable Membrane H Type Electrochemical Cell for Three Electrode Gas Aeration Experiments

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Standard & Customized Electrochemical Cells


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