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Optically Transparent Thin Layer Spectroelectrochemical Cell for In Situ UV Vis NIR Spectroscopic Analysis

Standard & Customized Electrochemical Cells

Optically Transparent Thin Layer Spectroelectrochemical Cell for In Situ UV Vis NIR Spectroscopic Analysis

Item Number : PL-DJ12

Price varies based on specs and customizations


Optical Path Length
1.0 mm (0.5 mm / 0.2 mm inserts available)
Spectral Range
200 nm to 2500 nm (UV-Vis-NIR)
Cuvette Material
High-Purity Far-UV Quartz (JGS1)
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Product Overview

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This advanced spectroscopic electrochemical cell is engineered to facilitate seamless in-situ UV-Vis and near-infrared (NIR) spectroelectrochemical analysis, bridging the gap between electronic structure transitions and electrochemical reaction kinetics. Designed to fit standard spectrophotometer sample compartments, the unit enables researchers to monitor spectroscopic variations simultaneously during dynamic electrochemical processes. The integrated thin-layer geometry ensures rapid, uniform electrolysis of the sample volume, minimizing diffusion-limited time delays and ensuring high-fidelity data acquisition.

Ideally suited for demanding industrial laboratories, academic institutions, and high-tech research centers, the system supports critical studies in electrocatalysis, redox polymer dynamics, organometallic chemistry, and energy storage systems. The robust construction provides the chemical compatibility required for organic solvents, highly corrosive media, and varying pH ranges, making it an indispensable tool for characterizing complex electrochemical pathways.

Built with the utmost precision, the equipment guarantees exceptional optical clarity and mechanical integrity under challenging testing conditions. By utilizing high-purity quartz and custom-machined fluoropolymer components, the design mitigates cross-contamination risks and maintains superior sealing performance. Industrial buyers can rely on this cell for consistent, highly reproducible spectral data, ensuring operational efficiency and long-term diagnostic confidence.

Key Features

  • Optically Transparent Thin-Layer Design: The system utilizes an ultra-thin optical path chamber to achieve rapid, near-instantaneous electrolysis of the sample volume under active potential control, which dramatically reduces diffusion lag and enables precise transient spectroscopic tracking.
  • Premium Quartz Cuvette Body: Crafted from optical-grade quartz, the outer cuvette features exceptional light transmittance with negligible distortion, ensuring that low-concentration analytes are accurately detected without background interference in the UV, visible, or NIR spectrums.
  • Precision CNC-Machined PTFE Cap: The custom-engineered polytetrafluoroethylene sealing lid provides unmatched resistance against aggressive organic solvents, strong acids, and bases, preventing evaporation and maintaining a strict, contamination-free environment during volatile test runs.
  • Integrated Multi-Electrode Configuration: The cell features pre-aligned ports for a high-area working electrode, a counter electrode, and a miniature reference electrode, guaranteeing stable electrical contact and optimal spatial distribution to prevent uncompensated resistance.
  • Universal Spectrophotometer Compatibility: Engineered to mimic standard cuvette dimensions, the apparatus easily mounts into standard cuvette holders across a broad range of commercial UV-Vis-NIR spectrophotometers without requiring custom optical rail modifications.
  • Minimized Sample Volume Requirement: By optimizing the inner thin-layer volume, this unit allows laboratories to conduct highly sophisticated analyses using minimal quantities of expensive or rare syntheses, reducing overall operational costs.
  • Leak-Proof Gas Purge Capabilities: Equipped with optional integrated purging channels within the fluoropolymer cap, the cell allows for effective deaeration of the solution using inert gas to eliminate dissolved oxygen interference during highly sensitive redox tests.
  • Durable, Disassemble-Friendly Construction: Every component is designed for swift disassembly and reassembly, facilitating thorough cleaning procedures, electrode replacement, and maintenance, thereby extending the system's operational lifespan in high-throughput environments.

Applications

Application Description Key Benefit
Electrocatalyst Evaluation In-situ monitoring of active catalyst surfaces during oxygen reduction (ORR) or hydrogen evolution reactions (HER). Enables real-time correlation between potential-driven structural shifts and catalytic reaction rates.
Redox Polymer Studies Tracking spectral changes in electrochromic and conducting polymers during doping and dedoping cycles. Delivers precise optical density profiles linked directly to specific oxidation and reduction potentials.
Organometallic Characterization Investigating oxidation states and charge-transfer kinetics in transition metal complexes and coordination compounds. Facilitates fast, uniform electrolysis to isolate and identify transient radical intermediates.
Battery Material Analysis Analyzing chemical changes within liquid battery electrolytes and electrode interfaces during simulated charging cycles. Provides deep diagnostic insight into electrolyte degradation pathways and solid-electrolyte interphase kinetics.
Bioelectrochemistry Research Evaluating redox behavior in proteins, enzymes, and cellular electron transport systems under controlled potentials. Minimizes denaturation risks with highly biocompatible, bio-inert quartz and fluoropolymer materials.
Dye & Pigment Development Studying color shifts, degradation paths, and degradation mechanisms of synthetic dye molecules in organic solutions. Delivers high-precision absorption profiles across a wide wavelength range under continuous voltage control.

Technical Specifications

The PL-DJ12 system is designed for high-resolution optical and electrochemical synchronization. Utilizing precision-engineered components, this model delivers reliable performance across various commercial spectrophotometer platforms.

Parameter PL-DJ12 Specification Detail Options / Remarks
Standard Optical Path Length 1.0 mm Optional 0.5 mm or 0.2 mm thin-layer inserts available
Outer Cuvette Dimensions 12.5 mm × 12.5 mm × 45.0 mm Standard footprint for universal cell holders
Spectral Range 200 nm to 2500 nm Far-UV Quartz (JGS1 equivalent) window material
Working Electrode (WE) Gold Mesh (99.99% purity) Interchangeable with Platinum Mesh or ITO Glass
Counter Electrode (CE) Platinum Wire (Ø 0.5 mm × 50 mm) Integrated pre-aligned port
Reference Electrode (RE) Miniature Ag/AgCl Electrode (Ø 2.0 mm) Saturated KCl type, low-leakage design
Cap / Lid Material Virgin High-Purity PTFE Custom multi-port CNC machined configuration
Active Electrolysis Volume 0.8 mL to 1.5 mL Minimizes consumption of precious target compounds
Chemical Compatibility Universal (Agonistic Solvents, Acids, Bases) Zero-swelling fluoropolymer and quartz construction
Operating Temperature -20°C to +120°C Robust seal integrity across thermal boundaries

Why Choose This Product

  • Premium Engineering Heritage: Crafted from ultra-pure, virgin fluoropolymer and JGS1 far-UV quartz, this cell offers superior structural stability and optical clarity compared to mass-produced alternatives.
  • Unmatched Machining Precision: KINTEK’s advanced end-to-end CNC machining capabilities ensure that electrode ports, cap fittings, and custom microfluidic channels line up with micron-level tolerance.
  • Proven Test-to-Test Consistency: Minimizing cell-to-cell variance ensures that researchers obtain identical background profiles, leading to highly reproducible datasets and publication-ready experimental results.
  • Flexible Customization Support: Because we control the manufacturing process from raw fluoropolymer blocks to finished units, we can modify path lengths, electrode materials, and lid layouts to match your unique experimental parameters.
  • Comprehensive Technical Guidance: Backed by an expert engineering support team, we provide direct assistance in configuring your optical setup, selecting compatible solvents, and maintaining electrode life.

Contact our technical sales team today to discuss your in-situ spectroelectrochemical requirements or to request a customized quote for your lab setup.

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Optically Transparent Thin Layer Spectroelectrochemical Cell for In Situ UV Vis NIR Spectroscopic Analysis

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Standard & Customized Electrochemical Cells


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