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Replaceable Membrane H Type Electrochemical Cell for Three Electrode Experiments with High Borosilicate Glass and PTFE Sealing Components

Standard & Customized Electrochemical Cells

Replaceable Membrane H Type Electrochemical Cell for Three Electrode Experiments with High Borosilicate Glass and PTFE Sealing Components

Item Number : PL-DJ02

Price varies based on specs and customizations


Chamber Volume
10 ml
Chamber Architecture
H-Type with Replaceable Membrane
Body Material
High Borosilicate Glass
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Product Overview

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This high-precision electrochemical cell system is specifically engineered to meet the demanding requirements of academic research and industrial laboratory investigations. Designed as a classic dual-chamber H-type configuration, this apparatus allows for the complete isolation of the cathodic and anodic chambers, preventing the crossover of reaction products while facilitating unimpeded ionic transport. The system features a modular membrane mounting assembly, which is ideal for evaluating ion-exchange membranes or conducting sensitive electrochemical reactions where product segregation is paramount.

The cell body is constructed from high-grade borosilicate glass, offering superior thermal shock resistance and optical clarity, which allows for visual monitoring of electrocatalytic processes or gas evolution. The chamber architecture includes a specialized hollow-layer profile that eliminates solution dead zones and blind spots, ensuring uniform solute concentrations and consistent kinetic conditions. With a standardized volume capacity of 10ml, this system is optimized for high-value catalysts, limited-volume liquid electrolytes, and precise analytical trials.

Built to support rigorous experimental designs, the system provides two distinct sealing options to cater to varying levels of air sensitivity: relative sealing for routine liquid-state analysis and absolute sealing for highly sensitive anaerobic electrochemistry. By co-locating the reference electrode and the working electrode within the same chamber, this equipment minimizes uncompensated solution resistance (IR drop), resulting in highly reproducible cyclic voltammetry and impedance data. This system stands as a testament to precision engineering, ensuring high performance under complex testing conditions.

Key Features

  • Dual-Chamber Membrane Interface: The system splits the reaction environment into distinct working and counter electrode compartments separated by an ion-exchange membrane. A heavy-duty chain clamp locks the chambers securely, enabling rapid membrane replacement while maintaining a hermetic, leak-proof barrier.
  • Optimized IR Drop Mitigation: The spatial layout of the glass chambers ensures that the reference electrode resides in the immediate vicinity of the working electrode. This reduces the uncompensated electrolyte resistance path, delivering superior potential control and highly accurate voltammetric sweeps.
  • High-Grade Borosilicate Glass Construction: Crafted from premium chemical-resistant borosilicate glass, the single-layer cell body incorporates a unique hollow geometry. This specialized structural design actively prevents solution entrapment and dead spaces, ensuring uniform electrochemical diffusion throughout the 10ml volume.
  • Precision-Engineered Internal Thread Glass Joints: The connection ports on the glass body utilize an internal thread design that interfaces seamlessly with high-purity fluoropolymer components. Tightening the threaded fittings compresses the O-ring seals, forming a highly secure joint without requiring vacuum grease.
  • Modular Sealing Options: Users can configure the cell for relative sealing using a compression screw mechanism on a solid polytetrafluoroethylene plug, or absolute hermetic sealing via a proprietary capped design with integrated inner-jack connectors.
  • Sub-Surface Gas Purging Array: Equipped with an integrated gas aeration tube that extends below the liquid level, the system permits efficient purging and saturation of the electrolyte. This design enables precise control over the atmospheric headspace and dissolved gas concentrations.
  • Customizable Extraction Ports: The glass cell body can be customized to include auxiliary sampling ports, allowing researchers to withdraw aliquots or introduce reagents mid-run. This functionality preserves the cell's internal environment while facilitating real-time kinetic analysis.
  • Chemically Inert Fluoropolymer Fittings: All seals, caps, and plugs are machined from high-performance fluoropolymers, ensuring absolute resistance to aggressive acids, strong bases, and organic solvents. This material choice prevents contamination and guarantees structural integrity over years of continuous laboratory use.

Applications

Application Description Key Benefit
Proton Exchange Membrane (PEM) Testing Evaluates the proton conductivity, chemical stability, and permeability of polymer electrolyte membranes under controlled potentials. Fast membrane swap-out with the integrated chain clamp minimizes downtime between runs.
Electrocatalytic CO2 Reduction Investigates gaseous reduction reactions where gaseous reactants must bubble directly into the liquid electrolyte under anaerobic conditions. Sub-surface aeration allows precise gas saturation while the absolute seal prevents oxygen ingress.
Water Splitting (HER/OER) Separates oxygen evolution at the anode from hydrogen evolution at the cathode to compute quantitative Faradaic efficiency. Strict physical chamber separation prevents gas mixing and ensures pure gas sample collection.
Electrosynthesis and Organic Electrochemistry Conducts synthetic transformations where anodic and cathodic intermediates must remain isolated to prevent reverse reactions. High borosilicate glass and pure PTFE construction resist aggressive organic solvents and strong acids.
Lithium-Ion Battery Electrolyte Characterization Analyzes the electrochemical window and transport numbers of novel non-aqueous liquid electrolytes in an air-free environment. Absolute hermetic seal with inner-jack electrode interfaces prevents volatile solvent evaporation and moisture contamination.
Biosensor and Kinetic Assays Performs cyclic voltammetry and impedance measurements on sensitive surface-bound enzymes or biochemical molecules. Co-located reference and working electrodes minimize IR drop, ensuring extremely low signal-to-noise ratios.

Technical Specifications

Parameter PL-DJ02-R (Relative Sealing Variant) PL-DJ02-A (Absolute Sealing Variant)
Base Model Number PL-DJ02 PL-DJ02
Chamber Configuration H-Type Dual Chamber H-Type Dual Chamber
Total Working Volume 10 ml 10 ml
Cell Body Material High Borosilicate Glass (Single Layer) High Borosilicate Glass (Single Layer)
Body Design Specialization Integrated hollow layer (eliminates solution blind spots) Integrated hollow layer (eliminates solution blind spots)
Chamber Connection Type Sealed chain clamp for easy membrane swap Sealed chain clamp for easy membrane swap
Membrane Separation Ion-Exchange Membrane (User-supplied) Ion-Exchange Membrane (User-supplied)
Electrode Setup Compatibility Three-electrode system (Requires elongated electrodes) Three-electrode system (Requires elongated electrodes)
Reference Electrode Placement Co-located in working electrode chamber (reduces IR drop) Co-located in working electrode chamber (reduces IR drop)
Glass Sealing Interface Internal thread design with PTFE compression Internal thread design with PTFE compression
Electrode Port Sealing Relative Sealing via PTFE plug with screw-compressed O-ring Absolute Sealing via PTFE cap with inner-jack connections
Gas Aeration System Sub-surface bubbling gas tube Sub-surface bubbling gas tube
Sampling Interface Optional custom sampling port (extra charge) Optional custom sampling port (extra charge)
Valve Integration Compatibility No valve option supported No valve option supported
Tubing Connection Compatibility Standard laboratory tubing Quick connectors for 3mm OD PTFE tubing

Why Choose This Product

  • Premium Material Integration: Utilizing high-grade borosilicate glass paired with KINTEK's precision CNC-machined fluoropolymer (PTFE) caps and fittings, this system guarantees absolute chemical resistance, preventing metal-ion contamination and preserving sample purity.
  • Uncompromising Atmospheric Integrity: Designed for researchers working with highly volatile or air-sensitive compounds, the absolute sealing variant utilizes internal headphone-jack style connections and quick-connect 3mm PTFE tube fittings to eliminate gaseous leakage entirely.
  • Scientific Excellence in Design: By deliberately positioning the reference electrode in the same chamber as the working electrode, the design minimizes uncompensated resistance. The hollow-layer glass architecture prevents solution blind spots, ensuring reproducible mass transport kinetics.
  • Modular Customization and Support: Backed by our end-to-end CNC machining capabilities, this system can be customized with additional sampling ports, thermowells, or tailored dimensions to fit your existing laboratory hardware and specialized experimental setups.

For more information on customized configurations, bulk ordering options, or to receive a tailored quotation for your specific laboratory requirements, please contact our technical sales team today.

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Product Datasheet

Replaceable Membrane H Type Electrochemical Cell for Three Electrode Experiments with High Borosilicate Glass and PTFE Sealing Components

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Standard & Customized Electrochemical Cells


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